Here is my logic for thinking it was a tip sealing issue
-the only thing that was affected was the low end. I didn't have problems with the upper area.
-The change was so drastic, I hard time believing anything else would cause that (subjective I know)
-Even when listening to them with the tips I had, I had trouble getting a good seal and I would constantly lose bass. I maybe should have measured them with my comply tips instead to see if that made a difference in repeatability measuring. When I finally switched to the complys for listening vs my too soft apple tips my sealing issues went away during listening sessions.
Now I am not ruling out connection issues, but higher impedance should affect treble and roll it off.
My current measurement rig is a Umm-6 with a clear vinyl tube, laptop soundcard, ATRA with MLS 32K. Ignore the white line, that was when I was seeing what the SRS setting did to my onboard soundcard. If you look at the two separate graphs you can see how I was having trouble at getting a consistent bass measurement